Module Catalogue 2013/14

CEG8625 : Chemical Analysis of Organic Matter

  • Offered for Year: 2013/14
  • Module Leader(s): Dr Geoffrey Abbott
  • Owning School: Civil Engineering & Geosciences
Semesters
Semester 1 Credit Value: 10
ECTS Credits: 5.0
Pre Requisites
Pre Requisite Comment

None, but a chemical or geochemical background

Co Requisites
Co Requisite Comment

-

Aims

The aim of this module is to give an overview of the basic analytical organic geochemical techniques employed in petroleum and organic geochemistry.

As a result of the chemical diversity and complexity of sedimentary organic matter, Petroleum Geochemistry makes use of innovative and sophisticated instrumentation and analytical methods. These will both be described in this module as together, these are capable of separating the complex mixtures of components observed in the geosphere as well as detecting, quantifying and most importantly, identifying minute amounts of information-rich molecules in both source rock extracts and crude oils.

Outline Of Syllabus

Sampling design and sample preparation (clean and crush)
Extraction of rocks
Introduction to fractionation of bitumen -Liquid column chromatography -Thin layer chromatography
Principles, nomenclature and types of Chromatography
Frontal analysis, displacement method, elution development
Theory and practise of liquid       chromatography
-Classical
-HPLC
Theory and practice of thin layer chromatography
Theory and practice of gas chromatography
Mass Spectrometry
-Principles
-Instrumentation
-Applications
Theory and practice of pyrolysis - gas chromatography and pyrolysis - GC-MS

Learning Outcomes

Intended Knowledge Outcomes

On completion of this module, students will be familiar with the fundamental theory of the chromatographic separation of complex mixtures. They will also have a strong grasp of the principles of mass spectrometry, an awareness of the main types of instruments used in petroleum geochemistry, their modes of application and the types of data that they produce. Lastly, they will be aware of some of the techniques involving pyrolysis which are used in petroleum geochemistry.

Intended Skill Outcomes

Students will be able to extract and fractionate complex mixtures of organic molecules from crude oils and other geological materials.

Graduate Skills Framework

Graduate Skills Framework Applicable: Yes
  • Cognitive/Intellectual Skills
    • Data Synthesis : Present
    • Numeracy : Assessed
    • Literacy : Assessed
    • Information Literacy
      • Source Materials : Present
      • Synthesise And Present Materials : Present
      • Use Of Computer Applications : Present
  • Self Management
    • Planning and Organisation
      • Decision Making : Present
    • Personal Enterprise
      • Initiative : Present
      • Problem Solving : Present
      • Adaptability : Present
  • Interaction
    • Communication
      • Interpersonal : Present
    • Team Working
      • Collaboration : Present

Teaching Methods

Teaching Activities
Category Activity Number Length Student Hours Comment
Guided Independent StudyAssessment preparation and completion15:005:00Project report
Guided Independent StudyAssessment preparation and completion11:301:30Exam
Guided Independent StudyAssessment preparation and completion10:450:45Class test.
Scheduled Learning And Teaching ActivitiesLecture91:009:00N/A
Guided Independent StudyAssessment preparation and completion91:009:00Revision for exam
Scheduled Learning And Teaching ActivitiesPractical66:0036:00N/A
Guided Independent StudyReflective learning activity112:0012:00Practical write-up.
Guided Independent StudyReflective learning activity12:152:15Revision for class test.
Guided Independent StudyReflective learning activity91:009:00Lecture write-up.
Guided Independent StudyIndependent study115:3015:30Includes background reading and reading lecture notes for a full understanding of material.
Total100:00
Teaching Rationale And Relationship

Specialist knowledge and understanding are primarily imparted via lecture classes, supported by computer-hosted reference materials. Subject specific skills are taught through hands-on laboratory practical classes.
Students are encouraged and expected to learn through reflection and independent reading. They are supported in this by the provision of an extensive, but prioritised, reading list. Observations and discussions during laboratory classes aid development of understanding whilst a short test at the end of the module (ten-minute-test) enables students to monitor the progress of their learning.
Subject specific skills are learnt through participation in, and reflection on, a lengthy series of laboratory practical classes.
Key skills are practised through participation in laboratory practical classes.

Reading Lists

Assessment Methods

The format of resits will be determined by the Board of Examiners

Exams
Description Length Semester When Set Percentage Comment
Written Examination901A60Unseen written examination.
Other Assessment
Description Semester When Set Percentage Comment
Report1M40Project report in form of scientific paper (approx. 2000 words).
Formative Assessments
Description Semester When Set Comment
Written exercise1MShort (10 minute) test
Assessment Rationale And Relationship

The specialist skills knowledge and understanding imparted during this module are assessed by means of unseen written examination and a written laboratory report. The written examination employs a range of approaches in order to accurately assess student abilities. These may include essay, calculation, data interpretation, and multi-part questions.

Timetable

Past Exam Papers

General Notes

N/A

Note: The Module Catalogue now reflects module information relating to academic year 13/14. Please contact your School Office if you require module information for a previous academic year.

Disclaimer: The University will use all reasonable endeavours to deliver modules in accordance with the descriptions set out in this catalogue. Every effort has been made to ensure the accuracy of the information, however, the University reserves the right to introduce changes to the information given including the addition, withdrawal or restructuring of modules if it considers such action to be necessary.