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Module

CHY1510 : Chemical Laboratory Skills 1

  • Offered for Year: 2020/21
  • Module Leader(s): Dr Zuleykha McMillan
  • Lecturer: Dr Cristina Navarro Reguero, Dr Toni Carruthers, Dr Johan Eriksson, Dr Hanno Kossen
  • Owning School: Natural and Environmental Sciences
  • Teaching Location: Newcastle City Campus
Semesters
Semester 1 Credit Value: 10
Semester 2 Credit Value: 10
ECTS Credits: 10.0

Aims

The aims of this module is to show students how the fundamental principles of scientific inquiry serve to advance knowledge. Students will learn to evaluate data and report results, and introduce the most fundamental techniques of chemical analysis and train students in the appropriate handling of scientific data.

Students will be taught basic aspects of safe laboratory practice and the ability to use safety information sources. The module will facilitate students to develop manipulative skills with items of laboratory apparatus that are commonly-encountered in the professional workplace, and provide a “hands-on”, contextualised, tangible perspective on chemical concepts taught elsewhere in the curriculum.

Outline Of Syllabus

This module trains chemical laboratory skills that are important in the chemical industry and in many other sectors of employment. The key skills taught span the sub-disciplines of physical, organic, inorganic and medicinal chemistry. The module provides a tangible, “hands-on” contextualisation of topics encountered elsewhere in Newcastle chemistry degrees. Skills and techniques taught within this module provide a foundation for the more advanced techniques encountered in subsequent Stages.

Students learn how the fundamental principles of scientific inquiry serve to advance knowledge. They learn to evaluate hypotheses and report on observations. Students develop strong familiarity with apparatus including flasks, pipettes, balances and burettes. They become familiar with common analytical techniques (spectroscopy, chromatography, melting point) and their advantages and limitations.

The syllabus includes;
• laboratory and safety awareness
• introduction to techniques of chemical separation, purification and synthesis
• introduction to techniques of chemical analysis (melting point, chromatography,
titration, gravimetric analysis)
• basic interpretation of infrared, UV-Visible and fluorescence spectra
• introduction to calorimetry, electrochemistry and spectroscopy.
• introduction to fundamental principles of calibration and data handling.

Teaching Methods

Please note that module leaders are reviewing the module teaching and assessment methods for Semester 2 modules, in light of the Covid-19 restrictions. There may also be a few further changes to Semester 1 modules. Final information will be available by the end of August 2020 in for Semester 1 modules and the end of October 2020 for Semester 2 modules.

Teaching Activities
Category Activity Number Length Student Hours Comment
Structured Guided LearningLecture materials160:308:00Online - pre-recorded short lectures to support material covered in practicals and dry labs
Guided Independent StudyAssessment preparation and completion44:0016:00Online tests on practical aspects
Guided Independent StudyAssessment preparation and completion48:0032:00Students complete their lab reports based on results of their experiments
Guided Independent StudyAssessment preparation and completion14:004:00Online - assessment of dry labs.
Guided Independent StudyDirected research and reading152:0030:00Online - module lecturer will give students relevant reading for module topics throughout semester
Scheduled Learning And Teaching ActivitiesPractical163:0048:002 x 3h practical session will take place every fortnight in the laboratory
Guided Independent StudySkills practice116:0016:00Students watch videoclips of techniques on CANVAS and complete relevant tests
Structured Guided LearningStructured non-synchronous discussion44:0016:00Discussion board on CANVAS
Scheduled Learning And Teaching ActivitiesWorkshops41:004:00Dry Lab zoom weekly session, first 4 weeks of Sem 1
Scheduled Learning And Teaching ActivitiesDrop-in/surgery141:0014:00Lab Q&A Zoom session
Guided Independent StudyIndependent study17:007:00Independent study
Scheduled Learning And Teaching ActivitiesModule talk51:005:00Induction lectures to 4 lab courses and 1 dry lab
Total200:00
Teaching Rationale And Relationship

Dry Labs provide the students with an opportunity to gain practice in basic chemical manipulations.

Practical sessions are designed to introduce students to key concepts and allow them the opportunity to develop expertise in a range of fundamental scientific skills, including using scientific literature, and collecting, interpreting and presenting scientific information.

Assessment Methods

Please note that module leaders are reviewing the module teaching and assessment methods for Semester 2 modules, in light of the Covid-19 restrictions. There may also be a few further changes to Semester 1 modules. Final information will be available by the end of August 2020 in for Semester 1 modules and the end of October 2020 for Semester 2 modules.

The format of resits will be determined by the Board of Examiners

Other Assessment
Description Semester When Set Percentage Comment
Practical/lab report1M20Single online assessment after 1st block of lab work
Practical/lab report1M20Single online assessment after 2nd block of laboratory work
Practical/lab report2M20Single online assessment after 3rd block of laboratory work
Practical/lab report2M20Single online assessment after 4th block of laboratory work
Practical/lab report1M20Dry Lab report
Zero Weighted Pass/Fail Assessments
Description When Set Comment
Practical/lab reportMSkills assessment of laboratory
Assessment Rationale And Relationship

Students will be expected to present notes of their practical work in their laboratory notebooks and use these notes to complete the summative reports.

The practical reports will assess the students’ ability to plan and carry out experimental work within the laboratory setting, and accurately record, analyse and report scientific data. In producing the report, students will need to demonstrate their use of taught practical skills, and appropriate reporting and interpretation of data.

The skills associated with recording scientific data are assessed by a mark for the notebook, which is kept during each laboratory. The outcomes of individual experiments are assessed by short templated submission and/or online methods - these tasks may be completed in laboratory hours.

There is one summative assessement of the drylab material and an in-laboratory practical examination at the end of the course.

Reading Lists

Timetable