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Module

CHY3510 : Chemical Laboratory Skills 3P (Inactive)

  • Inactive for Year: 2020/21
  • Module Leader(s): Dr Nick Walker
  • Owning School: Natural and Environmental Sciences
  • Teaching Location: Newcastle City Campus
Semesters
Semester 1 Credit Value: 10
Semester 2 Credit Value: 10
ECTS Credits: 10.0

Aims

The aim of this module is to:

• train students to apply the scientific method to investigate hypotheses. Activities are
investigative such that students structure their experiments with minimal formalised
instructions but while under supervision.
• train students in more advanced techniques of chemical analysis used in research laboratories.
For example, NMR spectroscopy and crystallography.
• Train students in the formal process of risk assessment and recording of hazard mitigation
actions.
• Teach strategic aspects of experimental investigations. For example, where multiple steps of
chemical synthesis are required which may require detailed planning.
• Provide a “hands-on”, contextualised, tangible perspective on advanced chemical concepts
taught elsewhere in the curriculum.

Outline Of Syllabus

This module trains chemical laboratory skills that are important in the chemical industry and in many other sectors of employment. The skills taught span the sub-disciplines of physical, organic and inorganic chemistry. The module provides a tangible, “hands-on” contextualisation of topics encountered elsewhere in Newcastle chemistry degrees. The module builds on knowledge and skills provided by the pre-requisite modules, Chemical Laboratory Skills Stage 1 and Stage 2.

This module requires students to think strategically about experiments having multiple parts. It requires that students structure their own investigations and reporting in the absence of detailed instructions. This module differs from Chemical Laboratory Skills 3M in having a significant physical chemistry component. The experiments that students undertake may vary from year-to-year while being appropriate for the contextualisation of material taught within the Organic, Inorganic and Physical Chemistry modules.

The syllabus includes;
• detailed planning of control measures and risk reporting when considering the safety of
experiments.
• strategic approaches toward challenges involving multi-step chemical syntheses.
• anhydrous and non-anhydrous experimental techniques
• interpretation of infrared, UV-Visible and fluorescence spectra to include detailed
numerical and/or graphical analysis of spectroscopic data.
• open-ended investigations where students choose between methodologies while testing
hypotheses.
• teaching of how to use the scientific literature (ie peer-reviewed sources) to inform
investigations and interpretations. Make comparisons with literature sources while aware
of experimental accuracy.

Teaching Methods

Please note that module leaders are reviewing the module teaching and assessment methods for Semester 2 modules, in light of the Covid-19 restrictions. There may also be a few further changes to Semester 1 modules. Final information will be available by the end of August 2020 in for Semester 1 modules and the end of October 2020 for Semester 2 modules.

Teaching Activities
Category Activity Number Length Student Hours Comment
Guided Independent StudyAssessment preparation and completion62:0012:00Reports covering all practical sessions
Scheduled Learning And Teaching ActivitiesLecture31:003:00Lectures
Scheduled Learning And Teaching ActivitiesPractical1510:00150:005 x 10h practical sessions for each of Inorganic (50h), Organic (50h) and Physical chemistry (50h)
Guided Independent StudyIndependent study135:0035:00Background reading
Total200:00
Teaching Rationale And Relationship

Competencies in practical classes, procedures, observation, record-keeping and report writing, will be taught, learnt and expected within these modules. Practicals will reinforce elements of the lectures and extend the practical techniques and experience that the students gained in Stage 2.

Assessment Methods

Please note that module leaders are reviewing the module teaching and assessment methods for Semester 2 modules, in light of the Covid-19 restrictions. There may also be a few further changes to Semester 1 modules. Final information will be available by the end of August 2020 in for Semester 1 modules and the end of October 2020 for Semester 2 modules.

The format of resits will be determined by the Board of Examiners

Other Assessment
Description Semester When Set Percentage Comment
Practical/lab report2M1006 practical reports covering all sections
Assessment Rationale And Relationship

Assessment of laboratory practicals will be summatively assessed through the completion of practical reports. These are designed to examine the student’s ability to present scientific information and data in a concise way while following a specific presentation format.

Students will be expected to present notes of their practical work in their laboratory notebooks and use these notes to complete the summative and formative exercises.

Reading Lists

Timetable